الجامعـــة الوطنيـــة الخاصـــة

Al-Wataniya Private University

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A Joint Scientific Research by Dr. Shuaib Al-Ahmad, the Dean of the Faculty of Pharmacy, with Other Researchers, in Baghdad Scientific Journa .. Scientific Research is A Common Goal

In an effort to promote a culture of scientific research among students and to work towards adopting a scientific approach as a main component in its educational plans, Al-Wataniya Private University has given significant attention and support to scientific research in all its forms. This has resulted in diverse research outputs that have been formulated by numerous doctors and professors from various faculties of the university. They believe in the role of scientific research in building exceptional students and its actual importance in serving both the local and international scientific community.

In this context, the Baghdad Science Journal published on 11/6/2023 a joint scientific research by Dr. Shuaib Al-Ahmad, Dean of the College of Pharmacy at Al-Wataniya Private University, along with Dr. Youssef Al-Ahmad and Professor Duaa Al-Hussein from the College of Pharmacy at Al-Baath University. The research titled ” Development and Validation of a Novel Analytical Method (Ion Pair HPLC) For Separating and Determining Bisoprolol Fumarate and Carvedilol in Pure and Their Pharmaceutical Forms.” focused on High-Performance Liquid Chromatography for the separation and detection of Bisoprolol Fumarate and Carvedilol in their raw materials and pharmaceutical forms.

The research was included in the Scopus database as a scientifically based study characterized by accuracy and clarity.

The aim of the joint scientific research is to show a new analytical method (ion pair HPLC) for the analysis of Bisoprolol Fumarate (BIS) and Carvedilol (CAR) in bulk and tablet. The developed analytical method has been carried out on an Inertsil ODS-3 5μL column 4.6 X 250 mm (w), as stationary phase using a mobile phase {Acetonitrile/ water 50/50 (v/v) containing sodium heptane sulfonic salt 0.001M as Ion pair agent}. The detection wavelength was 223 nm and the flow rate was 1.5 mL /min. Retention times were 3.5 min of BIS and 5.8 min of CAR. The analytical method has been validated by ICH guidelines. The developed method gave linearity in the concentration range of 20–60 μg/ mL accuracy with mean recovery values between 98-102 % (99.73% for BIS and 101.2% for CAR). The developed method is useful for separating and determining Bisoprolol Fumarate and Carvedilol in their pharmaceutical forms.

It is worth mentioning the continuous efforts made by Al-Wataniya Private University, represented by its presidency and deanships, to enhance the value of scientific research among doctors, professors, and student researchers due to its significant role in increasing their academic knowledge and refining their practical experiences in reality.

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